In an effort to reduce the modern carbon contamination, diatoms were separated from sediments, purified, and pre-oxidized by concentrated nitric and perchloric acids to permit dating of opal-intrinsic organic carbon approximately 0.
Several experiments designed to eliminate the modern C contamination were attempted, but so far we have not been able to obtain a radiocarbon age on mobile web dating username mills 14 C-dead Southern Ocean opal-rich sediments, either bulk TOC or purified diatom opal samples, as old as our procedural blank.
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